Course Syllabus for Fall 2012
CLASS SCHEDULE
Lecture: Tuesday and Thursday, 8:00 - 8:50 am; 109 Garrigus
Laboratory: Tuesday and Thursday, 9:00 - 10:50 am; 105 Garrigus
INSTRUCTOR
Luke Boatright, Ph.D.
Office: 412 Garrigus
Phone: 257-5988
E-mail: wlboat1@uky.edu Office Hours: Open
REQUIRED TEXTBOOK
"Food
Analysis, 4th edition,"
S.S. Nielsen, Ed., 2010. Springer, New York, NY.
GRADING SYSTEM
Evaluation | Cumulative Numerical Grade | Letter Grade | |||
Quizzes | 10% | Undergraduates | Graduates | ||
Exams | 50% | 90-100 | 92-100 | A | |
Lab Reports | 25% | 80-89 | 82-91 | B | |
Individual Projects | 10% | 70-79 | 72-81 | C | |
Class Participation | 5% | 60-69 | 62-71 | D | |
100% | Below 60 |
Below 62 |
E |
The numerical scale given here will be the guideline for assigning final grades in this course. The numerical scale may or may not be lowered in assigning the final grades, but will not be any higher than that indicated.
A quiz will be given about every week. The lowest quiz score will be discarded. The four exams will cover both lecture and lab material. The final exam, which is not comprehensive, is optional for undergraduate students.
Subject mater is best retained when students participate in classroom discussions and ask questions. In order to effectively participate in these discussions each reading assignment should be completed prior to the corresponding class period. Five percent of a students final grade will reflect their involvement in classroom discussions.
Missed quizzes and exams can be made up only if: a) Notification is given in advance of a justifiable absence, or b) An unanticipated, justifiable absence is verified. In accordance with the University rules governing absences, as provided by the University Senate Rules Sections V - 2.4.1 and 2.4.2 (http://www.uky.edu/StudentAffairs/Code/part2.html), an excess of each three (3) unexcused absences for lectures will result in a drop in the final letter grade for the class. Unexcused laboratory absences can not be made-up and will count as a zero (0) for that laboratory write-up. If a student has excussed absences in excess of one-fifth of the class contact hours, the student will be required to withdraw from the course (University Senate Rules Section V-5.2.4.2).
Instructions for the individual project are given on a separate sheet (note: graduate students cannot use any topic relating to their thesis for their class project). All assignments submitted by students should represent their own work and ideas unless appropriate recognition is given to the original author. University policies related to plagiarism can be found in your copy of Student Rights and Responsibilities or at http://www.uky.edu/StudentAffairs/Code/part2.html section 6.3.1. Any student whom the instructor has sufficient evidence to believe has cheated or plagiarized in the course will receive an automatic "E" (failure) in the entire course. There will be no exceptions.
Students will be informed of their current progress based on the criteria in the syllabus before the midterm date of the semester, term or session. (SR 6.1.3.A)
Students should provide one week notice to the instructor in order to arrange for accommodations due to a religious observance.
GENERAL INFORMATION
Chapters in the
required textbook will be assigned for each lecture. Students are
expected to read the assignment and be prepared to ask questions and
discuss the material
in lecture. Important course information is often discussed at
the beginning of
lecture, so please do not be late. There will be discussion in lecture
and lab concerning
the laboratory experiments. The laboratory procedures should be
brought to lecture
so they can be discussed during class before each lab. Students are to
arrive at the lab
well prepared to do the experiment. Some aspects of the experiment done
in lab (e.g.
Questions for Class Discussion from laboratory handout) will be
discussed in the following
lecture.
REFERENCES
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Official Methods of Analysis.
Association of Official Analytical Chemists, 15th ed. (1990). (on reserve or in reference section of the Agriculture Library). |
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Official Methods and Recommended Practices, American Oil Chemists' Society, 4th ed.(1987). |
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Food Analysis: Theory and Practice. Pomeranz and Meloan, 3rd. ed., (1994). |
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Food Chemistry. Fennema, (1985). |
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Food Analysis: Principles and Techniques. Gruenwedel and Whitaker, Vol. 1 (1984), Vol 2, (1984). |
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Food Composition and Analysis. Aurand, Woods and Wells, (1987). |
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The Merck Index. (in reference section of Agriculture Library) |
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Code of Federal Regulations (CFR) 21:Parts 100-169; 9: Parts 200-319.(http://www.access.gpo.gov/nara/cfr/cfr-table-search.html) |
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Nutritive Value of American Foods. USDA Agriculture Handbook, (1984). |
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Food composition and nutritional tables, CRC Press, (1994). |
COURSE DESCRIPTION
Application of quantitative and qualitative analysis used in the physical, chemical and instrumental examination of food products. A special emphasis is placed on the evaluation of methods and interpretation of results.
COURSE OBJECTIVES
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To identify the principles, purposes, and applications of techniques to the chemical and instrumental analysis of foods. |
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To identify appropriate methods for proximate analysis of food products. |
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To provide chemical and instrumental laboratory
experience for students in the Food Science curriculum. |
Food
Analysis
(FSC 535)
Tuesday and Thursday; Class, 8:00 - 8:50
Laboratory, 9:00 - 10:50
Lecture Topics
Date | Description | Reading |
August 23 | Introduction | |
August 28 | Titratable Acidity | Ch. 13 |
August 30 | Principles of Ultraviolet, Visible and Fluorescence Spectroscopy | Ch. 22, 23 |
September 4 | Moisture and Ash | Ch. 6, 7 |
September 6 | Mineral Analysis | Ch. 12, 25 |
September 11 | Principles of Chromatography | Ch. 27 |
September 13 | Liquid Chromatography | Ch. 28 |
September 18 | Gas-Liquid Chromatography | Ch. 29 |
September 20 | Oven Review | |
September 25 | Exam I | |
September 27 | Carbohydrate Analysis | Ch. 10 |
October 2 | Carbohydrate Analysis (Con't) | |
October 4 | Carbohydrate Analysis (Con't) | |
October 9 | Lipid Analysis | Ch. 8, 14 |
October 11 | Lipid Analysis (Con't) | |
October 16 | Lipid Analysis (Con't) | |
October 18 | Open Review | |
October 23 | Exam II | |
October 25 | Protein Analysis | Ch. 9, 15 |
October 30 | Protein Separation & Characterization | |
November 1 | Protein Separation & Characterization | |
November 6 | Protein Analysis Continued / Reading Assisgnment | |
November 8 | Vitamins | |
November 13 | Pigments | Ch. 11 & 32 |
November 15 | Open Review | |
November 20 | Exam III | |
November 22 | Holiday | Ch. 26 |
November 27 | Mass Spectrometry | |
November 29 | Sensory Analysis | |
December 4 | Immunoassays & Thermal Analysis | Ch. 17, 31 |
December 6 | Open Review | |
Final Exam, (IV) - Wednesday, December 12, 8:00 A.M. |
Laboratory Schedule
Date | Description | Report Due Date |
August 23 | Introduction and Searching the Literature | |
August 28 | Standard Solutions and Titratable Acidity | Sept. 11 |
August 30 | Principles of Spectroscopy, Dilutions and Standard Curves | Sept. 11 |
September 4 | Moisture and Total Ash | Sept. 18 |
September 6 | Traditional Mineral Analysis | Sept. 18 |
September 11 | Thin-Layer Chromatography | Sept. 27 |
September 13 | Liquid Chromatography | Sept. 27 |
September 18 | Gas-Liquid Chromatography | Sept. 27 |
September 20 | Individual Projects | |
September 25 | Exam I | |
September 27 | Carbohydrates Analysis | Oct. 11 |
October 2 | Carbohydrate Analysis Continued | Oct. 11 |
October 4 | Vitamin Analysis - Library Search | Oct. 18 |
October 9 | Lipid Analysis (Extract &FFA) | Oct. 25 |
October 11 | Lipid Analysis (Extract & Phos) | Oct. 25 |
October 16 | Lipid Oxidation | Oct. 25 |
October 18 | Individual Projects | |
October 23 | Exam II | |
October 25 | Protein Analysis | Nov. 15 |
October 30 | Protein Separation & Characterization | |
November 1 | Protein Separation & Characterization | Nov. 15 |
November 6 | Vitamin Analysis I | Nov. 22 |
November 8 | Vitamin Analysis II | |
November 13 | Pigment Analysis | Nov. 27 |
November 15 | Individual Projects | |
November 20 | Exam III | |
November 22 | Holiday | |
November 27 | Mass Spectrometry | Dec. 6 |
November 29 | Sensory Analysis | Dec. 6 |
December 4 | Individual Projects | |
December 6 | Presentation of Individual Projects | |
*Reports with same due date can be combined into one report |